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電沈積三維孔洞型非貴重金屬觸媒於陰離子交換膜電解水陽極端之應用

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摘要 IAbstract III誌謝 VIContents VIIList of Figures XIList of Tables XVIIIChapter 1 Introduction 11-1 Energy converting and storage 11-2 Hydrogen production via water electrolysis 21-2-1 Proton exchange membrane electrolysis 31-2-2 Anion exchange membrane electrolys

is 41-3 The reaction of water electrolysis 6Chapter 2 Literature Review 112-1 Non-precious metal catalysts 122-2 Co oxide-based catalysts 172-2-1 Hydrothermal and sintering method 182-2-2 Electrodeposition method 192-3 Main effect for catalyst design 212-3-1 Crystallinity

effect 212-3-2 Structure effect 222-3-3 Heteroatoms effect 24Chapter 3 Motivation 26Chapter 4 Experimental Instruments 294-1 Chemicals and instruments 294-2 Experimental 324-2-1 Preparation of CoOOH/Cu/Ni foam 324-2-2 Preparation of NiCu/Ni foam 334-2-3 Preparation of NiCu

P/Ni foam 344-3 Potentiostat 364-4 Electrochemical measurements 384-4-1 Linear sweep and cycle voltammetry (LSV and CV) 384-4-2 Turnover frequency (TOF) 394-4-3 Faraday efficiency (FE) 404-4-3 Anion exchange membrane for water electrolysis 404-5 X-ray diffraction Spectrometer (X

RD) 434-6 Transmission Electron Microscope (TEM) 464-7 X-ray Photoelectron Spectroscopy (XPS) 484-8 X-ray absorption spectroscopy (XAS) 504-9 Operando XAS setup 55Chapter 5 Operando identification of hydrangea-like and amorphous cobalt oxyhydroxide supported by thin-layer copper for o

xygen evolution reaction 565-1 Morphology of the catalysts 565-2 Characteristics of the catalysts 625-3 Electrochemical performance of the catalysts 685-4 Long-term stability of the catalysts on AEMEL 725-5 Operando analysis of the catalysts 75Chapter 6 Barnacle-like phosphorized n

ickel-copper porous catalysts for oxygen evolution reaction 816-1 Electrochemical performance of the catalysts 816-2 Morphology and characteristics of the catalysts 846-3 Characteristics of the catalysts 886-4 Long-term stability of the catalysts on AEMEL 97Chapter 7 Conclusion 987

-1 Operando identification of hydrangea-like and amorphous cobalt oxyhydroxide supported by thin-layer copper for oxygen evolution reaction 987-2 Barnacle-like phosphorized nickel-copper porous catalysts for oxygen evolution reaction 99References 100