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鉑鉬、鉑鋯和鉑鐵銥觸媒催化維他命C和多巴胺氧化行為之分析

為了解決EELS EDX的問題，作者蘇陳佳頤 這樣論述：

總目錄中文摘要 2總目錄 4圖目錄 9表目錄 12第一章 前言 131-1 維他命C與多巴胺 131-2 研究目的與動機 15第二章 文獻回顧 172-1 維他命 C 172-1-1 維他命 C 結構 172-1-2 維他命 C 之物化性質 182-1-3 維他命 C 之生理功能與應用 212-1-4 維他命 C 於溶液中之降解機制 212-1-4-1 維他命 C 於電極表面上之電氧化行為 242-1-4-2 於酸性與中性環境下之電氧化行為 242-1-4-3 直接電氧化之機制探討 242-1-4-4 分離吸附行為之探討 282-1-4-5 於鹼性環境中之電

氧化行為 292-1-4-6 第一個氧化波峰之機制探討 292-1-4-7 第二個氧化波峰之機制探討 312-2多巴胺 332-2-1 多巴胺結構 332-2-2 多巴胺的物化性質 362-2-3 多巴胺之生理功能與應用 372-3導電碳黑 372-4感測器之介紹 402-4-1電化學感測器之介紹 422-4-2 電化學感測器之分類 432-4-3 維他命C感測器之文獻 462-4-4 多巴胺之感測器之文獻 472-5電化學感測器之分析理論 472-5-1 循環伏安法 472-5-2 計時電流法 512-5-3 極限電流法 532-5-4 擴散方程式 57第

三章 實驗方法與步驟 623-1 實驗藥品與耗材 623-2 實驗設備與儀器 643-2 實驗步驟 653-2-1 配置藥品 653-2-2 觸媒油墨製作 663-2-3 製備程序及製程條件 683-3 電極之電化學分析 693-3-1 循環伏安法 693-3-2 極化曲線 703-3-2 應答曲線 713-4 電極觸媒之特性分析 713-4-1 能量散佈光譜儀 (Energy-dispersive X-ray , EDX) 713-4-2 熱重分析儀 (Thermogravimetric Analysis , TGA) 723-4-3 X-ray 繞射光譜儀(X

-ray diffractometer , XRD) 723-4-4 穿透式電子顯微鏡(Transmission Electron Microscope， 73TEM) 73第四章 結果與討論 734-1 鉑合金觸媒之特性分析 734-1-1 表面型態與TEM分析 734-1-2 EDS 分析 774-1-3 熱重分析 794-1-4 晶型結構 814-2 合金觸媒之維他命 C 感測 834-2-1 感測維他命 C 之循環伏安圖 834-2-2 感測維他命 C 之極化曲線 854-2-3 感測維他命 C 之應答曲線與濃度校正曲線 874-2-4 感測維他命 C 之應答

時間 914-2-5 感測維他命 C 之選擇性 934-2-6 PtMo感測維他命 C 之穩定性與再現性 954-2-7 PtMo維他命 C 感測器與文獻比較 974-3 合金觸媒之多巴胺感測 994-3-1 感測巴胺之循環伏安圖 994-3-2 感測多巴胺之極化曲線 1014-3-3 感測多巴胺之應答曲線與濃度校正曲線 1034-3-4 感測多巴胺之應答時間 1064-3-5感測多巴胺之選擇性 1084-3-6 PtMo感測多巴胺之穩定性與再現性 1104-2-7 PtMo多巴胺感測器與文獻比較 112第五章 結論 114參考文獻 115

柱狀氧化鋅雙機制表面電漿智慧光電傳感器應用

為了解決EELS EDX的問題，作者Akhilesh Kumar Gupta 這樣論述：

The demands of photonic sensor systems have been used for the production of sensor applications to study various methods for the synthesis and properties of metal oxide and its composites. This study shows the defectless zinc oxide (ZnO-NR), due to its high-temperature anneal and the constructed of

gold nanoparticles for combined plasmon- energy transport model, as a robust and tunable plasmontronic sensor system for the detection of rhodamine (R6G). A correlation has been established between annealing temperature and the defect level concerning the diameter and density of ZnO-NR. In addition

, the deposition of the gold layer over ZnO-NR via thermal evaporator exhibits plasmonic field improvement in the visible range, which is revived after short, rapid annealing treatment. This improvement is due to the wide surface of the sensing area of Rhodamine (R6G) molecules on the hexagonal rod

and robust plasmonic coupling between metal and ZnO which efficiently senses the fluorescence signal. The percentage of energy transmission capacity has gradually declined with a rise in the GNP size of 72.93, 67.52, and 47.86 %, leading to an increase in the gap between the donor and the receiver o

f 63.03, 67.25 and 82.49 Å, respectively. In other words, the performance of the PC-SET met the 1/d4 distance dependence model between the donor and the acceptor molecules with long-distance detection ranges from 46.95 to 120 Å. Moreover, we used the same substrate as above and modeled one of the no

vel principal component analysis (PCA) methods to improve SERS signals using a machine learning approach. Zinc oxide nanoarrays (ZnO-NAs) were synthesized here using a hydrothermal method followed by zinc oxide nucleation on ITO glass substrates using an oxidation furnace at 500° C. The surface morp

hology was improved by short rapid thermal annealingvi(S-RTA) followed by the deposition of a gold layer by a thermal evaporator. RTA is one of the therapies that can provide an effective forum for producing "hot spots" for SERS enhancement with fewer defects. The proposed Au/ZnO-NA SERS sensor show

ed a 1.15x107 enhancement factor (EF) through the R6G Raman probe and excellent uniformity over the entire surface. The PCA algorithm has been used to derive useful features and details from the SERS signal.Further, the quality of our life demands energy as one of the most essential tools, for now,

with applications in health care as well as electronic devices. Nevertheless, we have suggested a solution-processed ZnO-NR & ZnO-Polystyrene (ZnO-PS) composite for the production of the Triboelectric Nanogenerator (TENG) platform for potential self-propelled medical system applications. Besides, we

have tried to build a plasmonic TENG device that provides a new direction for the light effect sensor as well as a self-powered energy harvesting device for various future applications.